Technology Process of Heptalene
There total 3 articles about Heptalene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1,2,5,6,9,10-hexabromocyclododecane;
With
18-crown-6 ether; potassium tert-butylate;
In
tetrahydrofuran;
at -100 ℃;
With
potassium;
In
tetrahydrofuran;
With
iodine;
In
tetrahydrofuran;
DOI:10.1021/ol0362921
- Guidance literature:
-
With
trityl tetrafluoroborate; trimethylamine;
Yield given. Multistep reaction;
1.) CH2Cl2, 30 min, 2.) CHCl3, room temperature, 1 h;
DOI:10.1021/ja00522a034
- Guidance literature:
-
Aus 1,6-Methano<10>annulen '(3)' ueber mehrere Zwischenstufen;