Benzenamine, N,N-dimethyl-4-nitro-, N-oxide

Base Information

• Chemical Name: Benzenamine, N,N-dimethyl-4-nitro-, N-oxide
• CAS No.: 26492-31-9
• Molecular Formula: C8H10N2O3
• Molecular Weight: 182.179
• Mol file: 26492-31-9.mol

Synonyms:

Chemical Property of Benzenamine, N,N-dimethyl-4-nitro-, N-oxide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenamine, N,N-dimethyl-4-nitro-, N-oxide

There total 2 articles about Benzenamine, N,N-dimethyl-4-nitro-, N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

N,N-Dimethyl-4-nitroaniline (100-23-2) → p-nitro-N,N-dimethylaniline-N-oxide (26492-31-9)

Guidance literature:

With dihydrogen peroxide; methyltrioxorhenium(VII); In methanol; at 25 ℃; Rate constant;

DOI:10.1021/jo00110a042

Reference yield:

→ p-nitro-N,N-dimethylaniline-N-oxide (26492-31-9)

Guidance literature:

With methanol; silver(l) oxide; und Abdampfen des Loesungsmittels;

Reference yield: 100.0%

p-nitro-N,N-dimethylaniline-N-oxide (26492-31-9) → formaldehyd (50-00-0,30525-89-4,61233-19-0) + N,N-Dimethyl-4-nitroaniline (100-23-2)

Guidance literature:

With 1H-imidazole; meso-tetraphenylporphyrin iron(III) chloride; DMA-OCH₃; In chloroform; at 25 ℃; for 0.5h;

DOI:10.1016/S0040-4039(00)84329-4

upstream raw materials:

N,N-Dimethyl-4-nitroaniline

Downstream raw materials:

N,N-Dimethyl-4-nitroaniline

N-methyl(p-nitroaniline)

formaldehyd

N,N-Dimethyl-O-(4-nitro-phenyl)-hydroxylamine

Refernces

• 1、 Zhu, Zuolin,Espenson, James H.. "Kinetics and Mechanism of Oxidation of Anilines by Hydrogen Peroxide As Catalyzed by Methylrhenium Trioxide". . p. 1326 - 1332. Retrieved 2007/10/02.