113311-44-7Relevant articles and documents
gem-DIALKOXYLATION OF 2-ACETYLTHIOPHENES AND 2-ACETYLFURANS
Gordeeva, G. N.,Kalashnikov, S. M.,Popov, Yu. N.,Kruglov, E. A.,Imashev, U. B.
, p. 638 - 641 (2007/10/02)
Reaction of 2-acetyl-substituted thiophenes and furans with alkyl nitrites in the presence of the corresponding aliphatic alcohols and hydrochloric acid leads to the formation of linear acetals of thienyl- and furylglyoxals, whose structure was established by IR, UV, NMR spectroscopy, and mass spectrometry methods.The main paths of the dissociation of the molecules under electron impact were established.
