60199-37-3Relevant articles and documents
Mild synthesis of N -acylsulfenamides from arylamides and disulfides
Zhang, Xing-Song,Zhang, Xiao-Hong
, p. 89 - 94 (2016/01/25)
An efficient and new method was developed to synthesize N-acylsulfenamides via NaH-promoted sulfenylation of benzamides with readily available disulfides under mild conditions. A series of N-acylsulfenamides were easily obtained in moderate to high yields. Moreover, the obtained N-acylsulfenamides were used as thiolating reagents in the synthesis of sulfenylpyrroles and 3-sulfenylbenzofurans.
Efficient synthesis of N-acylarenesulfenamides by acylation of arenesulfenamides
Bao, Ming,Shimizu, Masao,Shimada, Shigeru,Tanaka, Masato
, p. 303 - 309 (2007/10/03)
Acylation of arenesulfenamides proceeds efficiently by using either perfluorocarboxylic anhydrides or acid chlorides in the presence of pyridine as a base at low temperatures to give N-acylarenesulfenamides. Some N-alkylcarbonyl derivatives exist with imidic acid tautomers in an aprotic solvent.
REACTION OF DIARYL DISULFIDES WITH N-CHLOROAMIDES OF CARBOXYLIC ACIDS
Levchenko, E. S.,Dubinina, T. N.,Budnik, L. V.
, p. 1875 - 1880 (2007/10/02)
In the reaction of diaryl disulfides with N-chlorocarboxamides arenesulfenyl chlorides and N-acylarenesulfenamides are formed initially.The subsequent reaction path is determined by the reaction of the latter with the N-chlorocarboxamides, and N-acylarenesulfinimidoyl chlorides, N,N'-diacylaryldiazasulfonium chlorides, or N,N'-diacylarenesulfinamidines are formed, depending on the ratio of the reagents and on the reaction conditions.
