71648-41-4Relevant articles and documents
Merrifield resin-C6H4CH2N 3P(MeNCH2CH2)3N: An efficient reusable catalyst for room-temperature 1,4-addition reactions and a more convenient synthesis of its precursor P(MeNCH
Venkat Reddy, Chinta Reddy,Verkade, John G.
, p. 3093 - 3096 (2008/02/07)
(Chemical Equation Presented) 1,4-Additions to a variety of Michael acceptors with a wide variety of donors were efficiently catalyzed at room temperature by the title reusable Merrifield resin-supported catalyst. Advantages of this catalyst include a sim
SYNTHESIS AND REACTIONS OF 1-AZASPIROCYCLES: 1-AZASPIRODECANE AND 1-AZASPIRONONANE RING SYSTEMS.
Bryce, Martin R.,Gardiner, John M.,Horton, Paul J.,Smith, Susan A.
, p. 116 - 124 (2007/10/02)
Nitrocyclohexane reacted with methyl acrylate in the presence of Triton-B to yield nitro-ester (4) which cyclised to spirolactam (5) on treatment with zinc in ethanolic hydrochloric acid.Lactam (5) was reduced to pyrrolidine (7) by lithium aluminium hydri