Technology Process of 1,3,2-Dioxaborinane, 2-(2,3-difluoro-4-propylphenyl)-5,5-dimethyl-
There total 6 articles about 1,3,2-Dioxaborinane, 2-(2,3-difluoro-4-propylphenyl)-5,5-dimethyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: LDA / tetrahydrofuran / 1.5 h / -78 °C
1.2: 96 percent / tetrahydrofuran / -78 - 20 °C
2.1: P2O5 / pentane
3.1: 46.3 g / H2 / PtO2 / pentane / 12 h / 760 Torr
4.1: n-BuLi / tetrahydrofuran / 0.25 h / -78 °C
4.2: tetrahydrofuran / -78 - 20 °C
5.1: aq. HCl / diethyl ether
6.1: 56.3 g / NgSO4 / tetrahydrofuran / 1 h
With
hydrogenchloride; n-butyllithium; hydrogen; phosphorus pentoxide; lithium diisopropyl amide;
platinum(IV) oxide;
In
tetrahydrofuran; diethyl ether; pentane;
DOI:10.1039/b212107g
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 46.3 g / H2 / PtO2 / pentane / 12 h / 760 Torr
2.1: n-BuLi / tetrahydrofuran / 0.25 h / -78 °C
2.2: tetrahydrofuran / -78 - 20 °C
3.1: aq. HCl / diethyl ether
4.1: 56.3 g / NgSO4 / tetrahydrofuran / 1 h
With
hydrogenchloride; n-butyllithium; hydrogen;
platinum(IV) oxide;
In
tetrahydrofuran; diethyl ether; pentane;
DOI:10.1039/b212107g
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: P2O5 / pentane
2.1: 46.3 g / H2 / PtO2 / pentane / 12 h / 760 Torr
3.1: n-BuLi / tetrahydrofuran / 0.25 h / -78 °C
3.2: tetrahydrofuran / -78 - 20 °C
4.1: aq. HCl / diethyl ether
5.1: 56.3 g / NgSO4 / tetrahydrofuran / 1 h
With
hydrogenchloride; n-butyllithium; hydrogen; phosphorus pentoxide;
platinum(IV) oxide;
In
tetrahydrofuran; diethyl ether; pentane;
DOI:10.1039/b212107g