Technology Process of C30H19BrN2
There total 8 articles about C30H19BrN2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium phosphate; copper(l) iodide; ethylenediamine;
In
toluene;
at 75 ℃;
for 12h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene / 4 h / 100 °C
2.1: triethyl phosphite / 6 h / 150 °C
3.1: caesium carbonate / copper(l) iodide / toluene / 50 °C
3.2: 14 h / Reflux
4.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C
4.2: 12 h / 20 °C
5.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol / 5 h / Reflux
6.1: triethyl phosphite / 6 h / 150 °C
7.1: potassium phosphate; ethylenediamine; copper(l) iodide / toluene / 12 h / 75 °C
With
potassium phosphate; copper(l) iodide; n-butyllithium; sodium carbonate; caesium carbonate; ethylenediamine; triethyl phosphite;
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethanol; hexane; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: caesium carbonate / copper(l) iodide / toluene / 50 °C
1.2: 14 h / Reflux
2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C
2.2: 12 h / 20 °C
3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol / 5 h / Reflux
4.1: triethyl phosphite / 6 h / 150 °C
5.1: potassium phosphate; ethylenediamine; copper(l) iodide / toluene / 12 h / 75 °C
With
potassium phosphate; copper(l) iodide; n-butyllithium; sodium carbonate; caesium carbonate; ethylenediamine; triethyl phosphite;
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethanol; hexane; toluene;