2-(1,3-Dioxolan-2-yl)furan

Base Information

• Chemical Name: 2-(1,3-Dioxolan-2-yl)furan
• CAS No.: 1708-41-4
• Molecular Formula: C7H8O3
• Molecular Weight: 140.139
• Hs Code.: 2932999099
• NSC Number: 97506
• DSSTox Substance ID: DTXSID30937835
• Nikkaji Number: J501.841B
• Wikidata: Q82914058
• Mol file: 1708-41-4.mol

Synonyms:2-(1,3-Dioxolan-2-yl)furan;1708-41-4;2-(furan-2-yl)-1,3-dioxolane;2-(2-Furyl)-1,3-dioxolane;furalane;Furfural Ethylene Acetal;dioxolanyl furan;NSC97506;furanyl 1,3-dioxolane;1,3-dioxolan-2-yl-furan;SCHEMBL509970;2-furan-2-yl-[1,3]dioxolane;DTXSID30937835;1,3-Dioxolane,2-(2-furanyl)-;BAA70841;MFCD00671520;NSC-97506;AKOS015855713;AB06753;2-(2-Furyl)-1,3-dioxolane, 98%;CS-0205296;D2417;D90060

Chemical Property of 2-(1,3-Dioxolan-2-yl)furan

Chemical Property:

• Vapor Pressure: 0.344mmHg at 25°C
• Melting Point: -41 °C
• Refractive Index: 1.485
• Boiling Point: 206.3 °C at 760 mmHg
• Flash Point: 90.6 °C
• PSA: 31.60000
• Density: 1.189g/cm³
• LogP: 1.32500
• Storage Temp.: ?20°C
• XLogP3: 0.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 140.047344113
• Heavy Atom Count: 10
• Complexity: 109

Purity/Quality:

98% ^*data from raw suppliers

2-(1,3-Dioxolan-2-yl)furan ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1COC(O1)C2=CC=CO2

Technology Process of 2-(1,3-Dioxolan-2-yl)furan

There total 5 articles about 2-(1,3-Dioxolan-2-yl)furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

furfural (98-01-1) + ethylene glycol (107-21-1) → 2-(furan-2-yl)-1,3-dioxolane (1708-41-4)

Guidance literature:

With montmorillonite K-10; In benzene; for 1h; Heating;

DOI:10.1039/a605661j

Reference yield: 76.0%

furfural (98-01-1) → 2-(furan-2-yl)-1,3-dioxolane (1708-41-4)

Guidance literature:

With toluene-4-sulfonic acid; In water; ethylene glycol; benzene;

Reference yield: 63.0%

furfural (98-01-1) + 2-chloro-ethanol (107-07-3) → 2-(furan-2-yl)-1,3-dioxolane (1708-41-4)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl-formamide; at -60 ℃; for 1.5h;

DOI:10.1021/ol0613113

upstream raw materials:

furfural

ethylene glycol

2,2,7,7-tetramethyl-3,6-dioxa-2,7-disilaoctane

2-chloro-ethanol

Downstream raw materials:

furfural

C₂₀H₁₈O₇

2-(5-benzyl-furan-2-yl)-[1,3]dioxolane

C₁₄H₁₂F₂O₅S

Refernces

• 1、 Torkler,Karataeva,Samitov,Kul'nevich. "1H NMR spectra, configuration, and conformations of 2-mono- and 2,4-disubstituted 1,3-dioxolanes". . p. 1217 - 1221. Retrieved 1981.
• 2、 Belokon, Yuri N.,Gak, Alexander,Khakina, Ekaterina,Khrustalev, Victor N.,Korlyukov, Alexander A.,Kuznetsova, Svetlana,Li, Han,Lobanov, Nikolai,Nelyubina, Yulia,North, Michael,Peregudov, Alexander S.,Riazanov, Vladimir,Zhereb, Vladimir. "Inhibition by Water during Heterogeneous Br?nsted Acid Catalysis by Three-Dimensional Crystalline Organic Salts". . p. 6364 - 6372. Retrieved 2021/10/20.
• 3、 -. "PRODUCTION OF BENZENE DERIVATIVES". Page/Page column 22. . Retrieved 2021/06/22.