Technology Process of 2,5-Dimethoxybenzene-1,3-diol
There total 16 articles about 2,5-Dimethoxybenzene-1,3-diol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: alcoholic-aqueous NaOH-solution / zuletzt bei 45grad
2: hydrochloric acid; glacial acetic acid / 65 - 70 °C
With
hydrogenchloride; sodium hydroxide; acetic acid;
DOI:10.1039/jr9290000074
- Guidance literature:
-
Multi-step reaction with 4 steps
1: acetic acid; nitric acid / 4 h / 40 °C
2: sodium dithionite / ethyl acetate; water / 20 °C
3: sodium hydroxide / ethanol / 20 °C / pH 8 - 9
4: hydrogen; palladium 10% on activated carbon / methanol / 8 h / 20 °C
With
sodium dithionite; palladium 10% on activated carbon; hydrogen; nitric acid; acetic acid; sodium hydroxide;
In
methanol; ethanol; water; ethyl acetate;
DOI:10.1016/j.ejmech.2017.09.046