N-ethyl(4-hexyl)aniline

Base Information

• Chemical Name: N-ethyl(4-hexyl)aniline
• CAS No.: 1422573-77-0
• Molecular Formula: C₁₄H₂₃N
• Molecular Weight: 205.343
• Mol file: 1422573-77-0.mol

Synonyms:N-ethyl(4-hexyl)aniline

Chemical Property of N-ethyl(4-hexyl)aniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-ethyl(4-hexyl)aniline

There total 2 articles about N-ethyl(4-hexyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N-(4-hexylphenyl)acetamide (20330-59-0) → N-ethyl(4-hexyl)aniline (1422573-77-0)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 6h; Reflux;

DOI:10.1007/s11172-012-0124-4

Reference yield:

hexylbenzene (1077-16-3) → N-ethyl(4-hexyl)aniline (1422573-77-0)

Guidance literature:

Multi-step reaction with 3 steps

1: aluminum (III) chloride / dichloromethane / Cooling with ice

2: acetic acid; sodium azide; sulfuric acid / 3 h / 60 - 70 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / Reflux

With aluminum (III) chloride; lithium aluminium tetrahydride; sodium azide; sulfuric acid; acetic acid; In tetrahydrofuran; dichloromethane; 2: |Schmidt Reaction;

DOI:10.1007/s11172-012-0124-4

Reference yield: 76.0%

N-ethyl(4-hexyl)aniline (1422573-77-0) → 2-bromo-4-hexyl-N-ethylaniline

Guidance literature:

With bromine; In acetic acid; at 20 ℃; for 1h;

DOI:10.1039/c7dt01009e

upstream raw materials:

hexylbenzene

N-(4-hexylphenyl)acetamide

Downstream raw materials:

2,2'-bipyridyl-6,6'-dicarboxylic acid N,N'-diethyl-N,N'-di(4-hexylphenyl)amide

C₄₀H₄₈Br₂N₄O₂

Refernces