C₅₉H₇₂O₁₀

Base Information

• Chemical Name: C₅₉H₇₂O₁₀
• CAS No.: 858676-96-7
• Molecular Formula: C₅₉H₇₂O₁₀
• Molecular Weight: 941.215
• Mol file: 858676-96-7.mol

Synonyms:C₅₉H₇₂O₁₀

Chemical Property of C₅₉H₇₂O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₉H₇₂O₁₀

There total 8 articles about C₅₉H₇₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C66H75Cl3O12 → C59H72O10 (858676-96-7)

Guidance literature:

With dmap; In toluene;

DOI:10.1021/ja052226d

Reference yield:

2-((2R,4R,6S)-6-(((4S,6S)-6-(((2R,4R,6S)-6-(((2R,4R,6R)-6-((E,3S,4S)-4-hydroxy-3,5-dimethylhex-1-enyl)-2-phenyl-1,3-dioxan-4-yl)methyl)-2-phenyl-1,3-dioxan-4-yl)methyl)-2,2-dimethyl-1,3-dioxan-4-yl)methyl)-2-phenyl-1,3-dioxan-4-yl)acetaldehyde (858676-73-0) → C59H72O10 (858676-96-7)

Guidance literature:

Multi-step reaction with 4 steps

1.1: LiHMDS / tetrahydrofuran / 0.25 h / -72 °C

1.2: 77 percent / tetrahydrofuran / -72 - 0 °C

2.1: aq. LiOH / methanol; tetrahydrofuran / 16 h / 20 °C

3.1: Et₃N / tetrahydrofuran / 1 h / 20 °C

4.1: 9.3 mg / DMAP / toluene

With dmap; lithium hydroxide; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; toluene;

DOI:10.1021/ja052226d

Reference yield:

12-[6-(6-{6-[6-(4-hydroxy-3,5-dimethyl-hex-1-enyl)-2-phenyl-[1,3]dioxan-4-ylmethyl]-2-phenyl-[1,3]dioxan-4-ylmethyl}-2,2-dimethyl-[1,3]dioxan-4-ylmethyl)-2-phenyl-[1,3]dioxan-4-yl]-dodeca-2,4,6,8,10-pentaenoic acid ethyl ester → C59H72O10 (858676-96-7)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. LiOH / methanol; tetrahydrofuran / 16 h / 20 °C

2: Et₃N / tetrahydrofuran / 1 h / 20 °C

3: 9.3 mg / DMAP / toluene

With dmap; lithium hydroxide; triethylamine; In tetrahydrofuran; methanol; toluene;

DOI:10.1021/ja052226d

upstream raw materials:

2-((2R,4R,6S)-6-(((4S,6S)-6-(((2R,4R,6S)-6-(((2R,4R,6R)-6-((E,3S,4S)-4-hydroxy-3,5-dimethylhex-1-enyl)-2-phenyl-1,3-dioxan-4-yl)methyl)-2-phenyl-1,3-dioxan-4-yl)methyl)-2,2-dimethyl-1,3-dioxan-4-yl)methyl)-2-phenyl-1,3-dioxan-4-yl)acetaldehyde

{6-[6-(6-{6-[4-(4-methoxy-benzyloxy)-3,5-dimethyl-hex-1-enyl]-2-phenyl-[1,3]dioxan-4-ylmethyl}-2-phenyl-[1,3]dioxan-4-ylmethyl)-2,2-dimethyl-[1,3]dioxan-4-ylmethyl]-2-phenyl-[1,3]dioxan-4-yl}-acetaldehyde

benzyl-(2-{6-[6-(6-{6-[4-(4-methoxy-benzyloxy)-3,5-dimethyl-hex-1-enyl]-2-phenyl-[1,3]dioxan-4-ylmethyl}-2-phenyl-[1,3]dioxan-4-ylmethyl)-2,2-dimethyl-[1,3]dioxan-4-ylmethyl]-2-phenyl-[1,3]dioxan-4-yl}-vinyl)-dimethyl-silane

2,2-dimethoxy-propane

Downstream raw materials:

RK-397

Refernces