3,4-diphenyl-adiponitrile

Base Information

• Chemical Name: 3,4-diphenyl-adiponitrile
• CAS No.: 18891-12-8
• Molecular Formula: C₁₈H₁₆N₂
• Molecular Weight: 260.338
• Mol file: 18891-12-8.mol

Synonyms:3,4-diphenyl-adiponitrile

Chemical Property of 3,4-diphenyl-adiponitrile

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,4-diphenyl-adiponitrile

There total 8 articles about 3,4-diphenyl-adiponitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.0%

cinnamonitrile (4360-47-8) → meso-3,4-diphenyladiponitrile (84679-83-4) + d,l-3,4-diphenyladiponitrile (18891-12-8,84679-83-4,86071-29-6,86117-67-1,108391-55-5) + 1-cyano-2-amino-3-Z/E-tetrahydrofurfuralydene-4,5-cis/trans-diphenylcyclopent-1-ene + dihydrocinnamonitrile (645-59-0)

Guidance literature:

With 4-chloro-n-butyric anhydride; In N,N-dimethyl-formamide; Further byproducts given; electrolysis at -1.5 to -1.8 V (TBAI);

Reference yield:

cinnamic nitrile (1885-38-7) + acetonitrile (75-05-8,26809-02-9) → C18H16N2 (1132799-51-9) + 3,4-diphenyl-adiponitrile (18891-12-8) + 3-phenylglutaronitrile (78533-73-0) + dihydrocinnamonitrile (645-59-0)

Guidance literature:

With N,N,N,N-tetraethylammonium tetrafluoroborate; at 24.84 ℃; Title compound not separated from byproducts.; Electrochemical reaction;

DOI:10.1071/CH08092

Reference yield:

2-cyano-3-phenylacrylic acid (1011-92-3) → 3,4-diphenyl-adiponitrile (18891-12-8)

Guidance literature:

With sodium amalgam; water; at 45 ℃;

upstream raw materials:

2-cyano-3-phenylacrylic acid

cinnamonitrile

water

cinnamic nitrile

Refernces

• 1、 Degrand, Chantal,Mora, Raymond,Lund, Henning. "Electrochemical Acylation and Carboxylation of Some Activated Olefins". . p. 429 - 436. Retrieved 2007/10/02.